![]() Different methods have been applied in pesticide analysis, among these methods based on chromatographic separation with mass spectrometric detection have been extremely useful methods for determination of pesticide residues. Much attention has been made in pesticide analysis to improve agricultural productivity and control these compounds in food and environmental samples. This paper reviews the methodology, advantages and disadvantages of different microextraction techniques used in the analysis of pesticide residues from fruits and vegetables. The combination of several novel microextraction techniques to gas chromatography (GC), liquid chromatography (LC) and capillary electrophoresis (CE) has helped in the analysis of pesticides residues in various food matrices with little or no interferences from the complex food matrices. The microextraction techniques have been developed, in order to reduce sample preparation time, improve sensitivity and selectivity as well as to corroborate the recent advances in the development of highly sensitive and efficient analytical instrumentations. ![]() It is focused on the simplifications, miniaturization and improvement and reduction in volume of sample and solvents used while maintaining high throughput performance. Modern trends in sample preparation and subsequent instrumental analysis are aimed towards reliable and accurate analysis of fruits and vegetables. The use of microextraction techniques for the analysis of pesticide residues in fruits, vegetables and other contaminants have become very popular due to its environmental friendly nature.
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